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Dushyant Patel LC-MS/MS Method

S.K.P.C.P.E.R., Kherva 38 M .Pharm. Thesis

10. TRIAL-

Symmetry C8,

150 × 4.6 mm,

5 µ

Methanol :

5 mM Amm.

formate

(80:20)

Aqueous

MQC &

External

spiked

MQC

peak shape was

good, ion

suppression was not

observed

11. TRIAL-

Symmetry C8,

150 × 4.6 mm,

5 µ

Methanol :

5 mM Amm.

formate

(80:20)

Linearity

& P&A

(Waters

Cartridge)

Within acceptance

criteria

12. TRIAL-

Symmetry C8,

150 × 4.6 mm,

5 µ

Methanol :

5 mM Amm.

formate

(80:20)

Linearity

& P&A

(Orochem

Cartridge)

Within acceptance

criteria

4.2.9 METHOD SUMMARY:

Biological matrix : Human plasma

Sample volume required : 0.1 ml

Anticoagulant : Heparin

Analyte : Gabapentin

Internal standard : Levetiracetam

Calibration curve range : GBP : 0.05 µg/ml to 6.00 µg/ml

Detection mode : Mass spectrometry

Analytical technique : Liquid chromatography- Mass

spectrometry

Sample treatment : Solid phase extraction

Quantitation method : Peak area ratio

Weighting factor for Calibration curve : 1/X

4.2.10 CHROMATOGRAPHIC CONDITIONS:

Chromatographic

mode

: Reversed phase

Isocratic/gradient

mode

: Isocratic

Tray temperature : 5°C

Injection volume : 5.0 µl

Column : Brand : symmetry

: Type : C8

1 2 ... 45 46 47 48 49 50 51 52 53 54 55 ... 92 93

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