Samsung RT34M Manual do Utilizador descarregar pdf (Página 22)

Dushyant Patel Review of Literature

S.K.P.C.P.E.R., Kherva 10 M .Pharm. Thesis

10. Automated microanalysis of

gabapentin in human serum by

high-performance liquid

chromatography with fluorometric

detection

HPLC Extraction method: PP

Derivatization reagent: o-

phthaldialdehyde reagent

Column: Waters 5 µ RP

column (10 cmx4.6 mm)

IS: 1-(aminomethyl)

cycloheptane acetic acid

MP: 0.02 M phosphate buffer

(pH 4.5):ACN (50:50, v/v)

Detection : Fluorimetry

(EX: 230 nm, EM: 420 nm)

11. Determination of gabapentin in

plasma by high-performance liquid

chromatography

HPLC Derivatization reagent: o-

phthalaldehyde-3-

mercaptopropionic acid

IS: [1-(aminomethyl)-

cycloheptaneacetic acid

Column: Beckman

Ultrasphere 5 microns RP

MP: 0.33 M acetate buffer

(pH 3.7): methanol : ACN

(40:30:30, v/v/v)

Detection method :

Fluorimetry

(EX: 330 nm, EM: 440 nm)

12. Optimization of an HPLC method

for determination of gabapentin in

dosage forms through derivatization

with 1-fluoro-2, 4-dinitrobenzene

HPLC IS: Amlodipine

Derivatization reagent : 1-

fluoro-2,4-dinitrobenzene

Column : Nova-Pak C(18)

MP: ACN: sodium

dihydrogenphosphate (pH 2.5;

0.05 M) (70:30, v/v)

Detection: UV( 360 nm)

1 2 ... 17 18 19 20 21 22 23 24 25 26 27 ... 92 93

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