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Dushyant Patel List of Figures

S.K.P.C.P.E.R., Kherva IV M .Pharm. Thesis

List of Figures

Figure

No.

Title

Page

No.

4.1 Schematic diagram of mass spectroscopy 20

4.2 ESI process in the positive ion polarity mode 23

4.3 APCI process in the positive ion polarity mode 25

4.4

Schematic diagram of tandem mass spectrometer using triple quadrupole

instrument

4.5 Tuning spectrum of GBP & LEV 36

4.6 Representative chromatogram of blank plasma 51

4.7

Representative chromatogram of zero standard

4.8 Representative chromatogram of LLOQ 51

4.9 Representative chromatogram of ULOQ 52

4.10 Representative chromatogram of LQC 52

4.11 Representative chromatogram of MQC 52

4.12 Representative chromatogram of HQC 52

4.13 Representative calibration curve of GBP 54

5.1 Optimization of pH of buffer for (A) GBP-BCG (B) GBP-BTB complex 71

5.2

Optimization of volume of buffer for (A) GBP-BCG (B) GBP-BTB

complex

5.3 Representative spectra of GBP-BCG showing λmax at 416 nm 72

5.4 Representative spectra of GBP-BTB showing λmax at 421 nm 73

5.5 Calibration curve for GBP-BCG 74

5.6 Calibration curve for GBP-BTB 75

1 2 ... 5 6 7 8 9 10 11 12 13 14 15 ... 92 93

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